4-Cyanophenylacetic acid → HCID 23302727, compound

HRID 1953244Notes

Reaction equation

HRID 1953244 reaction equation
Cl.[C:2]1([NH:8][S:9]([C:12]2[CH:19]=[CH:18][C:15]([NH:16][CH3:17])=[C:14]([NH2:20])[CH:13]=2)(=[O:11])=[O:10])[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[C:21]([C:23]1[CH:28]=[CH:27][C:26]([CH2:29][C:30](O)=O)=[CH:25][CH:24]=1)#[N:22]>P(Cl)(Cl)(Cl)=O>[C:2]1([NH:8][S:9]([C:12]2[CH:19]=[CH:18][C:15]3[N:16]([CH3:17])[C:30]([CH2:29][C:26]4[CH:27]=[CH:28][C:23]([C:21]#[N:22])=[CH:24][CH:25]=4)=[N:20][C:14]=3[CH:13]=2)(=[O:10])=[O:11])[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

4

Reactant 2

HCID 795874-Cyanophenylacetic acidHCID 23302464HCID 23302464, compound

Product 1

HCID 23302727HCID 23302727, compound

Reagents, catalysts & solvents 1

HCID 24813Phosphorus oxychlorideSolvent

Procedure

Prepared analogously to Example 1a from 4-phenylaminosulphonyl-2-amino-N-methyl-aniline-hydrochloride and 4-cyano-phenylacetic acid in phosphorus oxychloride.

Sources & evidence

ORD record
ord-1f2e78570328479bb918877179a7184e
Source dataset
uspto-grants-2000_09
Patent number
US06114532

Reaction notes

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