HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → 1-N-methyl-4-nitrobenzene-1,2-diamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | 2-Fluoro-5-nitroaniline | HCID 67785 | — |
| Solvent | Water | HCID 962 | — |
| Product | 1-N-methyl-4-nitrobenzene-1,2-diamine | HCID 3420025 | — |
Reaction Steps
12.5 g (0.079 mol) of 2-fluoro-5-nitroaniline and 100 ml methylamine (40% in water) are stirred for 48 hours at ambient temperature. The precipitated product is diluted with water, suction filtered, washed and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06114532 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-2ca6a4af2d80489d9e179091655bcd52 |
| Source note | uspto-grants-2000_09 |