Methylamine → 1-N-methyl-4-nitrobenzene-1,2-diamine

HRID 1953260Notes

Reaction equation

HRID 1953260 reaction equation
F[C:2]1[CH:8]=[CH:7][C:6]([N+:9]([O-:11])=[O:10])=[CH:5][C:3]=1[NH2:4].[CH3:12][NH2:13]>O>[CH3:12][NH:13][C:2]1[CH:8]=[CH:7][C:6]([N+:9]([O-:11])=[O:10])=[CH:5][C:3]=1[NH2:4]

Participants

4

Reactant 2

HCID 6329MethylamineHCID 677852-Fluoro-5-nitroaniline

Product 1

HCID 34200251-N-methyl-4-nitrobenzene-1,2-diamine

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

12.5 g (0.079 mol) of 2-fluoro-5-nitroaniline and 100 ml methylamine (40% in water) are stirred for 48 hours at ambient temperature. The precipitated product is diluted with water, suction filtered, washed and dried.

Workup

  1. filtrationfiltered
  2. washwashed
  3. customdried

Sources & evidence

ORD record
ord-2ca6a4af2d80489d9e179091655bcd52
Source dataset
uspto-grants-2000_09
Patent number
US06114532

Reaction notes

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