Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | 4-CHLOROPHENYL CYCLOHEXYL KETONE | HCID 11579456 | — |
| Product | HCID 23302428 | HCID 23302428 | — |
Reaction Steps
To 50 ml fuming nitric acid are added batchwise at -25° C. 6.4 g (28.8 mmol) of 4-(cyclohexylcarbonyl)-chlorobenzene. The solution is stirred for 10 minutes at -25° C. and then poured onto ice water. The precipitated product is suction filtered, washed with water and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06114532 |
|---|
| Source dataset | uspto-grants-2000_09 |
|---|
| ORD ID | ord-e42da1b638a24a9ab3d1135ed5ef6b17 |
|---|
| Source note | uspto-grants-2000_09 |
|---|
