HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromopentane → HCID 54238531, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromopentane | HCID 8057 | — |
| Reactant | Phosphonic acid, (p-chlorophenyl)-, diethyl ester | HCID 200625 | — |
| Product | HCID 54238531 | HCID 54238531 | — |
Reaction Steps
3.5 g (15 mmol) of diethyl(4-chlorophenyl)-phosphonate and 3 ml (24.7 mmol) of n-pentylbromide are heated to 150° C. for 90 minutes with stirring. The cooled clear solution is chromatographed on silica gel and eluted with cyclohexane/ethyl acetate (7:3 to 1:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06114532 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-c3c4d82bcb9b4d94b1ebe9cead0112e1 |
| Source note | uspto-grants-2000_09 |