HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53720842, compound → HCID 23297275, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53720842 | HCID 53720842 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 23297275 | HCID 23297275 | 111.1% |
Reaction Steps
50 mL of a THF solution containing 3.79 g (8.69 mmol) of 6-decanoyl-1,2,3,4-tetrahydro-2-naphthalenecarboxylic acid benzyl ester and 0.43 g of 5% palladium/carbon was placed in a hydrogen atmosphere, using a baloon, and was stirred at room temperature for 24 hours. The reaction mixture was filtered and by concentrating the filtrate, there was obtained 3.19 g of 6-decanoyl-1,2,3,4-tetrahydro-2-naphthalenecarboxylic acid. The yield was 100%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06117359 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-6b2f66643ed04e0382b52a2ca7c7441a |
| Source note | uspto-grants-2000_09 |