HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 18364483, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 4670734 | HCID 4670734 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 18364483 | HCID 18364483 | — |
Reaction Steps
Thionyl chloride (1.48 g, 11 mmol) was added to a solution of tris(2,4,6-trimethylphenyl)bismuthine (Example 14) (5.66 g, 10 mmol) in hexane (100 ml) at ambient temperature. The mixture was stirred for one hour and the precipitated product was isolated and recrystalized from ethanol. Yield: 5.70 g (90%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06117412 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-767109a18ab04cbabcea6df251a1658d |
| Source note | uspto-grants-2000_09 |