HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15372233, compound → HCID 23298081, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15372233 | HCID 15372233 | — |
| Reactant | HCID 23298086 | HCID 23298086 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23298081 | HCID 23298081 | 85.4% |
Reaction Steps
A suspension of 2-[3-[(E)-2-(6-acetamido-3-pyridyl)vinyl]phenylamino]-3-aminopyridine (1.5 g) and 3-pyridylpyruvic acid (0.79 g) in ethanol (30 ml) was stirred under reflux for 8 hours. The cold reaction mixture was filtered and washed with ethanol to give 2-(3-pyridylmethyl)-3-oxo-4-[3-[(E)-2-(6-acetamido-3-pyridyl)vinyl]phenyl]-3,4-dihydropyrido[2,3-b]pyrazine as colorless crystals (1.76 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06117875 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-8fdde0154cca4d099ca8d48b480a8d8e |
| Source note | uspto-grants-2000_09 |