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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1953416Generated: November 3, 2026

HCID 15372233, compound → HCID 23298081, compound

https://huagongshe.com/reaction/1953416

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 15372233HCID 15372233—
ReactantHCID 23298086HCID 23298086—
SolventEthanolHCID 702—
ProductHCID 23298081HCID 2329808185.4%

Reaction Steps

A suspension of 2-[3-[(E)-2-(6-acetamido-3-pyridyl)vinyl]phenylamino]-3-aminopyridine (1.5 g) and 3-pyridylpyruvic acid (0.79 g) in ethanol (30 ml) was stirred under reflux for 8 hours. The cold reaction mixture was filtered and washed with ethanol to give 2-(3-pyridylmethyl)-3-oxo-4-[3-[(E)-2-(6-acetamido-3-pyridyl)vinyl]phenyl]-3,4-dihydropyrido[2,3-b]pyrazine as colorless crystals (1.76 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06117875
Source datasetuspto-grants-2000_09
ORD IDord-8fdde0154cca4d099ca8d48b480a8d8e
Source noteuspto-grants-2000_09