HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23298448, compound → HCID 23298401, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23298448 | HCID 23298448 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 23298401 | HCID 23298401 | — |
Reaction Steps
To 6-nitro-1-(phenylmethyl)aminoindane hydrochloride (1.34 g, 4.40 mmol) in MeOH (100 ml) was added a catalytic amount of 10% Pd/C. The mixture was hydrogenated at 50 psi for 1 hr, filtered through celite, and concentrated to give 6-amino-1-(phenylmethyl)aminoindane hydrochloride which was homogeneous by TLC and used immediately in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06117898 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-09312a3dd6634c059253d40ef9e27857 |
| Source note | uspto-grants-2000_09 |