HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54189558, compound → HCID 23297809, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54189558 | HCID 54189558 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23297809 | HCID 23297809 | — |
Reaction Steps
A solution of t-butyl 4-[N-(t-butoxycarbonyl)-N-(isopentyl)amino-methyl]-3-nitrobenzoate (2.27 mmol) in ethanol (100 mL) containing 10% palladium on carbon (0.5 g) was hydrogenated (40 psi). After 30 min, the mixture was filtered and concentrated to give t-butyl 3-amino-4-[N-(t-butoxycarbonyl)-N-(isopentyl)-aminomethyl]benzoate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06117866 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-d42657b1eded415db88e860a6bbcb04d |
| Source note | uspto-grants-2000_09 |