HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluoro-2-methyl-6-nitroaniline → HCID 23297976, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluoro-2-methyl-6-nitroaniline | HCID 10374842 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 23297976 | HCID 23297976 | — |
Reaction Steps
25 g (0.147 mol) of 4-fluoro-2-methyl-6-nitroaniline in 250 ml of tetrahydrofuran are hydrogenated at about 34° C. for 2 hours in the presence of 8 g of Raney nickel. The reaction mixture is then filtered off and concentrated. The title compound is obtained as a brown oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06117873 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-6a9a47c2f2b24015a1fcf9fa351f4736 |
| Source note | uspto-grants-2000_09 |