HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Acrylate → HCID 18533163, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Acrylate | HCID 7294 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Methoxybenzenethiol | HCID 12765 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 18533163 | HCID 18533163 | 100% |
Reaction Steps
4-Methoxythiophenol (4.80 g) was added to a stirred solution of methyl acrylate (3.08 ml) in dichloromethane (60 ml) at 0° C. Potassium carbonate (4.72 g) was added and the mixture was allowed to warm to room temperature overnight. The mixture was filtered over a plug of Celite® and the solvent was removed in vacuo to give the title compound as a yellow liquid (7.70 g, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06118001 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-c555bad20252496eb4371bd3a2d2cab6 |
| Source note | uspto-grants-2000_09 |