HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid monohydrate → 2-isopropylidene-1-indanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid monohydrate | HCID 521998 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 2-isopropylidene-1-indanone | HCID 1513334 | — |
Reaction Steps
The reaction mixture was dissolved in 300 ml of benzene and 4.2 g of p-toluenesulfonic acid monohydrate was added to the solution and refluxed for 2 hours for component distillation. The product was used in the subsequent reaction without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06121182 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-ec9a2c624181455a96b4fab23f811200 |
| Source note | uspto-grants-2000_09 |