huagongshe.com
HRID1954341

反应详情

EQUATION

反应方程式

HRID 1954341 的结构方程式

REACTANTS

反应物

2
结构：O=C(CCl)N1CCOCC1
HCID74040

2-Chloro-1-(morpholin-4-yl)ethanone

C6H10ClNO2

结构：CCOC(=O)c1c2ccc(CC(=O)NO)ccc-2c(C(=O)OCC)c1N.[Na]
HCID86755843

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)c1c2ccc(CC(=O)NOCC(=O)N3CCOCC3)ccc-2c(C(=O)OCC)c1N
HCID15411821

未命名化合物

收率 33%

PROCEDURE

实验过程

In an analogous manner to that described in Example 1, from diethyl 2-amino-6-[(hydroxycarbamoyl)-methyl]-azulene-1,3-dicarboxylate sodium and N-chloroacetyl-morpholine the title compound of m.p. 196-198° C. is obtained in 33% yield.