HRID1954343

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID10898

2-Bromo-1-ethanol

C2H5BrO

结构：CCOC(=O)c1c2ccc(CC(=O)NO)ccc-2c(C(=O)OCC)c1N.[Na]

HCID86755843

未命名化合物

PRODUCTS

生成物

结构：CCOC(=O)c1c2ccc(CC(=O)NOCCO)ccc-2c(C(=O)OCC)c1N

HCID15411825

未命名化合物

收率 15%

PROCEDURE

实验过程

In an analogous manner to that described in Example 1, from diethyl 2-amino-6-[(hydroxycarbamoyl)-methyl]-azulene-1,3-dicarboxylate sodium and 2-bromoethanol the title compound of m.p. 190-192° C. is obtained in 15% yield.