Hydrochloric Acid → HCID 23296417, compound

HRID 1954358Notes

Reaction equation

HRID 1954358 reaction equation
[CH2:1]([O:3][C:4]([CH2:6][N:7]1[C:11]2[CH:12]=[C:13]([N:16]([S:22]([CH3:25])(=[O:24])=[O:23])[CH2:17][CH2:18][N:19]([CH3:21])[CH3:20])[CH:14]=[CH:15][C:10]=2[N:9]=[C:8]1[CH2:26][O:27][C:28]1[CH:33]=[CH:32][C:31]([C:34]#[N:35])=[CH:30][CH:29]=1)=[O:5])[CH3:2].Cl.C(=O)([O-])[O-].[NH4+:41].[NH4+]>C(O)C>[CH2:1]([O:3][C:4]([CH2:6][N:7]1[C:11]2[CH:12]=[C:13]([N:16]([S:22]([CH3:25])(=[O:24])=[O:23])[CH2:17][CH2:18][N:19]([CH3:21])[CH3:20])[CH:14]=[CH:15][C:10]=2[N:9]=[C:8]1[CH2:26][O:27][C:28]1[CH:29]=[CH:30][C:31]([C:34](=[NH:41])[NH2:35])=[CH:32][CH:33]=1)=[O:5])[CH3:2]

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 517111Ammonium CarbonateHCID 23296481HCID 23296481, compound

Product 1

HCID 23296417HCID 23296417, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Prepared analogously to Example 1e from 1-ethoxycarbonylmethyl-2-[(4-cyanophenyl)-oxymethyl]-6-[N-(2-dimethylaminoethyl)-methanesulphonylamino]-benzimidazole and ethanolic hydrochloric acid, ethanol and ammonium carbonate.

Sources & evidence

ORD record
ord-405680a943674e63826dadd8f10c8e6a
Source dataset
uspto-grants-2000_09
Patent number
US06121308

Reaction notes

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