Hydrochloric Acid → HCID 23296454, compound

HRID 1954369Notes

Reaction equation

HRID 1954369 reaction equation
[CH3:1][N:2]1[C:6]2[CH:7]=[CH:8][C:9]([N:11]([S:18]([C:21]3[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=3)(=[O:20])=[O:19])[CH2:12][C:13]([O:15][CH2:16][CH3:17])=[O:14])=[CH:10][C:5]=2[N:4]=[C:3]1[C:27]([O:30][C:31]1[CH:36]=[CH:35][C:34]([C:37]#[N:38])=[CH:33][CH:32]=1)([CH3:29])[CH3:28].Cl.C(=O)([O-])[O-].[NH4+:44].[NH4+]>C(O)C>[CH3:1][N:2]1[C:6]2[CH:7]=[CH:8][C:9]([N:11]([S:18]([C:21]3[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=3)(=[O:20])=[O:19])[CH2:12][C:13]([O:15][CH2:16][CH3:17])=[O:14])=[CH:10][C:5]=2[N:4]=[C:3]1[C:27]([O:30][C:31]1[CH:36]=[CH:35][C:34]([C:37](=[NH:44])[NH2:38])=[CH:33][CH:32]=1)([CH3:28])[CH3:29]

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 517111Ammonium CarbonateHCID 23296577HCID 23296577, compound

Product 1

HCID 23296454HCID 23296454, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Prepared analogously to Example 1e from 1-methyl-2-[1-(4-cyanophenoxy)-1-methyl-ethyl]-5-[N-(ethoxycarbonylmethyl)-benzenesulphonylamino]-benzimidazole and ethanolic hydrochloric acid, ethanol and ammonium carbonate.

Sources & evidence

ORD record
ord-0d4dcf862bb240a58ee13786c765725b
Source dataset
uspto-grants-2000_09
Patent number
US06121308

Reaction notes

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