Hydrochloric Acid → HCID 53825809, compound

HRID 1954370Notes

Reaction equation

HRID 1954370 reaction equation
[CH3:1][N:2]1[C:6]2[CH:7]=[CH:8][C:9]([N:11]([S:17]([C:20]3[CH:21]=[CH:22][CH:23]=[C:24]4[C:29]=3[N:28]=[CH:27][CH:26]=[CH:25]4)(=[O:19])=[O:18])[CH2:12][C:13]([O:15][CH3:16])=[O:14])=[CH:10][C:5]=2[N:4]=[C:3]1[CH2:30][O:31][C:32]1[CH:37]=[CH:36][C:35]([C:38]#[N:39])=[CH:34][CH:33]=1.Cl.C(=O)([O-])[O-].[NH4+:45].[NH4+]>CO>[CH3:1][N:2]1[C:6]2[CH:7]=[CH:8][C:9]([N:11]([S:17]([C:20]3[CH:21]=[CH:22][CH:23]=[C:24]4[C:29]=3[N:28]=[CH:27][CH:26]=[CH:25]4)(=[O:19])=[O:18])[CH2:12][C:13]([O:15][CH3:16])=[O:14])=[CH:10][C:5]=2[N:4]=[C:3]1[CH2:30][O:31][C:32]1[CH:33]=[CH:34][C:35]([C:38](=[NH:45])[NH2:39])=[CH:36][CH:37]=1

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 517111Ammonium CarbonateHCID 70275333HCID 70275333, compound

Product 1

HCID 53825809HCID 53825809, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Prepared analogously to Example 1e from 1-methyl-2-[(4-cyanophenyl)-oxymethyl]-5-[N-(methoxycarbonylmethyl)-quinoline-8-sulphonylamino)-benzimidazole and methanolic hydrochloric acid, methanol and ammonium carbonate.

Sources & evidence

ORD record
ord-28ab5398a8bb4e9798e58d5c3399141f
Source dataset
uspto-grants-2000_09
Patent number
US06121308

Reaction notes

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