Hydrochloric Acid → HCID 23296432, compound

HRID 1954372Notes

Reaction equation

HRID 1954372 reaction equation
[CH2:1]([O:3][C:4]([CH2:6][CH2:7][CH2:8][N:9]1[C:13]2[CH:14]=[CH:15][C:16]([NH:18][S:19]([C:22]3[CH:23]=[CH:24][CH:25]=[C:26]4[C:31]=3[N:30]=[CH:29][CH:28]=[CH:27]4)(=[O:21])=[O:20])=[CH:17][C:12]=2[N:11]=[C:10]1[CH2:32][O:33][C:34]1[CH:39]=[CH:38][C:37]([C:40]#[N:41])=[CH:36][CH:35]=1)=[O:5])[CH3:2].Cl.C(=O)([O-])[O-].[NH4+:47].[NH4+]>C(O)C>[CH2:1]([O:3][C:4]([CH2:6][CH2:7][CH2:8][N:9]1[C:13]2[CH:14]=[CH:15][C:16]([NH:18][S:19]([C:22]3[CH:23]=[CH:24][CH:25]=[C:26]4[C:31]=3[N:30]=[CH:29][CH:28]=[CH:27]4)(=[O:21])=[O:20])=[CH:17][C:12]=2[N:11]=[C:10]1[CH2:32][O:33][C:34]1[CH:39]=[CH:38][C:37]([C:40](=[NH:47])[NH2:41])=[CH:36][CH:35]=1)=[O:5])[CH3:2]

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 517111Ammonium CarbonateHCID 23296556HCID 23296556, compound

Product 1

HCID 23296432HCID 23296432, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Prepared analogously to Example 1e from 1-(3-ethoxycarbonylpropyl)-2-[(4-cyanophenyl)-oxymethyl]-5-(quinoline-8-sulphonylamino)-benzimidazole and ethanolic hydrochloric acid, ethanol and ammonium carbonate.

Sources & evidence

ORD record
ord-0ecea13af3ee471889f6946e1e6f3659
Source dataset
uspto-grants-2000_09
Patent number
US06121308

Reaction notes

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