Hydrochloric Acid → HCID 53949378, compound

HRID 1954376Notes

Reaction equation

HRID 1954376 reaction equation
[CH3:1][N:2]1[C:6]2[CH:7]=[CH:8][C:9]([NH:11][S:12]([C:15]3[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=3)(=[O:14])=[O:13])=[CH:10][C:5]=2[N:4]=[C:3]1[CH2:21][O:22][C:23]1[CH:28]=[CH:27][CH:26]=[C:25]([C:29]#[N:30])[CH:24]=1.Cl.C(=O)([O-])[O-].[NH4+:36].[NH4+]>C(O)C>[CH3:1][N:2]1[C:6]2[CH:7]=[CH:8][C:9]([NH:11][S:12]([C:15]3[CH:16]=[CH:17][CH:18]=[CH:19][CH:20]=3)(=[O:14])=[O:13])=[CH:10][C:5]=2[N:4]=[C:3]1[CH2:21][O:22][C:23]1[CH:28]=[CH:27][CH:26]=[C:25]([C:29](=[NH:36])[NH2:30])[CH:24]=1

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 517111Ammonium CarbonateHCID 23296405HCID 23296405, compound

Product 1

HCID 53949378HCID 53949378, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Prepared analogously to Example 1e from 1-methyl-2-[(3-cyanophenyl)-oxymethyl]-5-(benzenesulphonylamino)-benzimidazole and ethanolic hydrochloric acid, ethanol and ammonium carbonate.

Sources & evidence

ORD record
ord-61d0e3dfa9e94dc48ccfbe25200614e4
Source dataset
uspto-grants-2000_09
Patent number
US06121308

Reaction notes

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