Hydrochloric Acid → HCID 23296441, compound

HRID 1954408Notes

Reaction equation

HRID 1954408 reaction equation
[CH3:1][N:2]1[C:6]2[CH:7]=[CH:8][C:9]([N:11]([S:13]([C:16]3[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=3)(=[O:15])=[O:14])[CH3:12])=[CH:10][C:5]=2[N:4]=[C:3]1[CH2:22][NH:23][C:24]1[CH:29]=[CH:28][C:27]([C:30]#[N:31])=[CH:26][C:25]=1[O:32][CH3:33].Cl.C(=O)([O-])[O-].[NH4+:39].[NH4+]>C(O)C>[CH3:1][N:2]1[C:6]2[CH:7]=[CH:8][C:9]([N:11]([S:13]([C:16]3[CH:17]=[CH:18][CH:19]=[CH:20][CH:21]=3)(=[O:15])=[O:14])[CH3:12])=[CH:10][C:5]=2[N:4]=[C:3]1[CH2:22][NH:23][C:24]1[CH:29]=[CH:28][C:27]([C:30](=[NH:39])[NH2:31])=[CH:26][C:25]=1[O:32][CH3:33]

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 517111Ammonium CarbonateHCID 23296634HCID 23296634, compound

Product 1

HCID 23296441HCID 23296441, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Prepared analogously to Example 1e from 1-methyl-2-[N-(4-cyano-2-methoxy-phenyl)-aminomethyl]-5-(N-methyl-benzenesulphonylamino)-benzimidazole and ethanolic hydrochloric acid, ethanol and ammonium carbonate.

Sources & evidence

ORD record
ord-1510cd3482ce4120b0c35feb5a2b133e
Source dataset
uspto-grants-2000_09
Patent number
US06121308

Reaction notes

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