Sodium Iodide → HCID 54106803, compound

HRID 1954465Notes

Reaction equation

HRID 1954465 reaction equation
Cl[CH2:2][Si:3]([CH3:11])([CH3:10])[C:4]1[O:5][CH:6]=[CH:7][C:8]=1[CH3:9].[I-:12].[Na+]>CC(=O)CC>[I:12][CH2:2][Si:3]([CH3:11])([CH3:10])[C:4]1[O:5][CH:6]=[CH:7][C:8]=1[CH3:9]

Participants

4

Reactant 2

HCID 5238Sodium IodideHCID 53771943HCID 53771943, compound

Product 1

HCID 54106803HCID 54106803, compound

Reagents, catalysts & solvents 1

HCID 6569Methyl Ethyl KetoneSolvent

Procedure

Reflux chloromethyl(dimethyl)(3-methyl-2-furyl)silane (114.5 mmol) in butanone (200 mL) containing sodium iodide (116 mmol) for 4 h, according to the procedure described in Example 1, step b to provide the title compound.

Sources & evidence

ORD record
ord-91116109051f4cc588ead74bdd0a8639
Source dataset
uspto-grants-2000_09
Patent number
US06121463

Reaction notes

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