HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15491191, compound → HCID 15491198, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15491191 | HCID 15491191 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 15491198 | HCID 15491198 | 85.2% |
Reaction Steps
A solution of the product from Example 1 (2.00 g, 4.71 mmol) in 100 mL of methanol was shaken with 20% Pd/C (0.25 g) on a Parr apparatus under a H2 atmosphere (50 psi) for 21 hours. The reaction mixture was filtered and the filtrate concentrated to give the title compound (1.64 g, 85%) as a white foam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06124280 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-0dbd8ad7b82842c6a8b86aa3f0de940c |
| Source note | uspto-grants-2000_09 |