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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1954692Generated: November 1, 2026

HCID 15491191, compound → HCID 15491198, compound

https://huagongshe.com/reaction/1954692

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 15491191HCID 15491191—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 15491198HCID 1549119885.2%

Reaction Steps

A solution of the product from Example 1 (2.00 g, 4.71 mmol) in 100 mL of methanol was shaken with 20% Pd/C (0.25 g) on a Parr apparatus under a H2 atmosphere (50 psi) for 21 hours. The reaction mixture was filtered and the filtrate concentrated to give the title compound (1.64 g, 85%) as a white foam.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06124280
Source datasetuspto-grants-2000_09
ORD IDord-0dbd8ad7b82842c6a8b86aa3f0de940c
Source noteuspto-grants-2000_09