HRID1954881

反应详情

EQUATION

反应方程式

REACTANTS

反应物

$反应SMILES：NC(=O)/C=C1\CCc2ccc(F)cc21$

HCID9837001

未命名化合物

$反应SMILES：O=C(Cl)/C=C1\CCc2ccc(F)cc21$

HCID15491026

未命名化合物

PRODUCTS

产物

$反应SMILES：NC(=O)/C=C1\CCc2cc(F)ccc21$

HCID10954366

未命名化合物

收率 44%

PROCEDURE

实验过程

This compound was prepared in a similar manner to that described for (E)-2-(6-fluoro-1-indanylidene)acetamide Example 1k by substituting (E)-2-(5-fluoro-1-indanylidene)acetyl chloride (3.16 g, 0.015 mol) for (E)-2-(6-fluoro-1-indanylidene)acetyl chloride. Recrystallization from acetonitrile:water mixtures gave 1.28 g (44%) of (E)-2-(5-fluoro-1-indanylidene)acetamide as a white solid; m.p., 191-193° C.

WORKUP

后处理

customThis compound was prepared in a similar manner to that
customRecrystallization from acetonitrile