HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1954994Generated: November 2, 2026
Ethyl nitroacetate → HCID 59896635, compound
https://huagongshe.com/reaction/1954994
Participants
| Role | Name | HCID | Charge |
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| Reactant | Ethyl nitroacetate | HCID 69379 | — |
| Reactant | HCID 22450336 | HCID 22450336 | — |
| Product | HCID 59896635 | HCID 59896635 | 57.3% |
Reaction Steps
A mixture of 1.4 g (0.0061 mole) of S-methyl-N-(6-chloro-3-pyridylmethyl)-N'-methylisothiourea obtained in Example 64 (2) and 2.7 g of ethyl nitroacetate was stirred with heating at 75-80° C. for 3 hours. After cooling, the crystals were collected by filtration, washed with CH3CN and dried. The procedure gave 1.1 g of the title compound as white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06124297 |
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| Source dataset | uspto-grants-2000_09 |
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| ORD ID | ord-a921c96a180f4c6894a49e86ed7d0073 |
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| Source note | uspto-grants-2000_09 |
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