HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloroethyl chloroformate → HCID 23294174, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloroethyl chloroformate | HCID 12305 | — |
| Reactant | HCID 15388763 | HCID 15388763 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 23294174 | HCID 23294174 | — |
Reaction Steps
According to the procedure indicated in Example 1a, 8-(2-amino-6-methylbenzylamino)-3-chloro-2-methylimidazo[1,2-a]pyridine (0.27 g) and 2-chloroethyl chloroformate (0.18 g) in dichloromethane (30 ml) give the title compound as a brown oil, which is used directly for further reaction in 2b.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06124313 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-e06463c5b7f941ebbfb8d1dad48d1911 |
| Source note | uspto-grants-2000_09 |