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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1955245Generated: November 1, 2026

Potassium Carbonate → HCID 23294434, compound

https://huagongshe.com/reaction/1955245

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
Reactant7-(Benzyloxy)naphthalen-2-olHCID 2763818—
ReactantHCID 22320730HCID 22320730—
SolventTetrahydrofuranHCID 8028—
ProductHCID 23294434HCID 23294434—

Reaction Steps

The title compound was prepared from 7-benzyloxy-naphthalen-2-ol (1.00 g, 4.00 mmol), 1-(4-benzyl-piperidin-1-yl)-2-bromo-ethanone (1.20 g, 4.05 mmol) and potassium carbonate (1.10 g, 7.96 mmol) in tetrahydofuran (40 ml) in three steps as a solid, mp 159-160° C. Analysis calculated for C24H27NO2 ·0.16H2O: C, 79.11; H, 7.56; N, 3.85. Found: C, 79.11; H. 7.63; N, 3.83.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06124323
Source datasetuspto-grants-2000_09
ORD IDord-20fa12c1c0384c1ea4c11de886bde26c
Source noteuspto-grants-2000_09