HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 23294434, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 7-(Benzyloxy)naphthalen-2-ol | HCID 2763818 | — |
| Reactant | HCID 22320730 | HCID 22320730 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 23294434 | HCID 23294434 | — |
Reaction Steps
The title compound was prepared from 7-benzyloxy-naphthalen-2-ol (1.00 g, 4.00 mmol), 1-(4-benzyl-piperidin-1-yl)-2-bromo-ethanone (1.20 g, 4.05 mmol) and potassium carbonate (1.10 g, 7.96 mmol) in tetrahydofuran (40 ml) in three steps as a solid, mp 159-160° C. Analysis calculated for C24H27NO2 ·0.16H2O: C, 79.11; H, 7.56; N, 3.85. Found: C, 79.11; H. 7.63; N, 3.83.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06124323 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-20fa12c1c0384c1ea4c11de886bde26c |
| Source note | uspto-grants-2000_09 |