HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 9799901, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 9799902 | HCID 9799902 | — |
| Reactant | HCID 9861328 | HCID 9861328 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 9799901 | HCID 9799901 | — |
| Product | HCID 9799902 | HCID 9799902 | — |
Reaction Steps
Ethyl 4-[3-(2-azabicyclo[2.2 2]octan-2-yl)propoxy]phenylpropiolate (compound 11) was prepared from compound 10 according to the method of example 2, then compound 11 was treated with HCl in ethyl ether in accordance with the method of example 1 (c). Ethyl 4-[3-(2-azabicyclo[2.2.2]octan-2-yl) propoxy]phenylpropiolate hydrochloride (compound 12) was obtained as a pale yellow crystal. The physical data is shown as follows.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06124460 |
| Source dataset | uspto-grants-2000_09 |
| ORD ID | ord-5ebe737c00214fa987b162ee97c80916 |
| Source note | uspto-grants-2000_09 |