HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butanol → HCID 19070340, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butanol | HCID 6386 | — |
| Reactant | 1,2-Benzenedicarbonitrile, 3-nitro- | HCID 162652 | — |
| Product | HCID 19070340 | HCID 19070340 | 70% |
Reaction Steps
As in Synthesis Example 1 but using 1.73 grams of 1,2-dicyano-3-nitrobenzene and 2.20 grams of t-butylalcohol, there was obtained 1.40 grams of 1,2-dicyano-3-t-butoxybenzene (yield of 70%). Next, as in Synthesis Example 1 but using 1.40 grams of this benzene compound and 0.58 gram of BBr3, there was obtained 2.9 grams of the end product (yield 60%, mp 184°-186° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05776656 |
| Source dataset | uspto-grants-1998_07 |
| ORD ID | ord-9cc55b70107143f6ba1c1477386ca616 |
| Source note | uspto-grants-1998_07 |