HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-tert-Butylcyclohexanol → HCID 19070338, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-tert-Butylcyclohexanol | HCID 26068 | — |
| Reactant | 1,2-Benzenedicarbonitrile, 4-nitro- | HCID 97443 | — |
| Product | HCID 19070338 | HCID 19070338 | 50% |
Reaction Steps
As in Synthesis Example 1 but using 1.73 grams of 1,2-dicyano-4-nitrobenzene and 4.7 grams of 2-t-butylcyclohexanol, there was obtained 1.41 grams of 1,2-dicyano-4-(2-t-butylcyclohexyloxy)benzene (yield of 50%). Next, as in Synthesis Example 1 but using 1.41 grams of this compound and 0.42 gram of BBr3, there was obtained 0.77 gram of the end product (yield 50%, mp 162°-165° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05776656 |
| Source dataset | uspto-grants-1998_07 |
| ORD ID | ord-8de19d7aee81442b981c0dad23c212ed |
| Source note | uspto-grants-1998_07 |