HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Bis(cyclohexylmethyl)-5,6-diaminouracil → HCID 178499795, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Bis(cyclohexylmethyl)-5,6-diaminouracil | HCID 22244975 | — |
| Reactant | (E)-methyl 4-(dimethoxymethyl)cinnamate | HCID 23247180 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 178499795 | HCID 178499795 | — |
Reaction Steps
(E)-Methyl 4-(dimethoxymethyl)cinnamate (from step (a)) was used in place of 4-formylcinnamic acid in the procedure described in step (d) of Example 1, except that a drop of acetic acid was added during the formation of the Schiff base with 1,3-bis(cyclohexylmethyl)-5,6-diaminouracil. Title compound was formed as a white powder, m.p. >270° C.; 1H-NMR (DMSO-d6) consistent with structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05776940 |
| Source dataset | uspto-grants-1998_07 |
| ORD ID | ord-d70e95ffe9e6466a86212f1b31b8ec61 |
| Source note | uspto-grants-1998_07 |