HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1'-Carbonyldiimidazole → HCID 19071300, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | Cycloheptylmethylamine | HCID 19071321 | — |
| Product | HCID 19071300 | HCID 19071300 | 24% |
Reaction Steps
In the manner of step (a) of Example 6, cycloheptanemethylamine hydrochloride (R. B. Turner and R. H. Garner, J. Amer. Chem. Soc. 1958, 80:1424-1430; 22.00 g, 0.135 mole) was reacted with 1,1'-carbonyldiimidazole to give 1,3-bis(cycloheptylmethyl)urea as a white powder (4.45 g, 24%), m.p. 106°-108° C.; 1H-NMR (DMSO-d6) consistent with structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05776940 |
| Source dataset | uspto-grants-1998_07 |
| ORD ID | ord-a84ebbf1e3b74be286b5f14623a0538a |
| Source note | uspto-grants-1998_07 |