HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methyl-1H-indol-1-amine → HCID 19072374, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methyl-1H-indol-1-amine | HCID 12427292 | — |
| Reactant | 3,4-Dichloropyridine--hydrogen chloride (1/1) | HCID 19072364 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 19072374 | HCID 19072374 | — |
Reaction Steps
The title compound was prepared from 3-methyl-1H-indol-1-amine and 3,4-dichloropyridine hydrochloride in isopropanol at 80° C. for 5 hours in substantially the same manner as in Example 17. Recrystallized from ethanol, m.p. 278°-280° C. (dec.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05776955 |
| Source dataset | uspto-grants-1998_07 |
| ORD ID | ord-f88951566b2f4c96909563de7d49e711 |
| Source note | uspto-grants-1998_07 |