m-Chloroperbenzoic acid → HCID 54018478, compound

HRID 1955713Notes

Reaction equation

HRID 1955713 reaction equation
ClC1C=CC=C(C(OO)=[O:9])C=1.[CH3:12][O:13][C:14]1[CH:15]=[C:16]2[C:20](=[CH:21][CH:22]=1)[C:19](=[CH:23][C:24]1[CH:29]=[CH:28][C:27]([S:30]([CH3:32])=[O:31])=[CH:26][CH:25]=1)[C:18]([CH3:33])=[C:17]2[CH2:34][C:35]([OH:37])=[O:36]>CC(C)=O>[CH3:12][O:13][C:14]1[CH:15]=[C:16]2[C:20](=[CH:21][CH:22]=1)[C:19](=[CH:23][C:24]1[CH:29]=[CH:28][C:27]([S:30]([CH3:32])(=[O:9])=[O:31])=[CH:26][CH:25]=1)[C:18]([CH3:33])=[C:17]2[CH2:34][C:35]([OH:37])=[O:36]

Participants

4

Reactant 2

HCID 70297m-Chloroperbenzoic acidHCID 53948779HCID 53948779, compound

Product 1

HCID 54018478HCID 54018478, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

5-methoxy-2-methyl-1-(p-methylsulfonylbenzylidene)-3-indenylacetic acid is prepared by the addition of 1.0 mol of m-chloroperbenzoic acid per mol of 5-methoxy-2-methyl-1-(p-methylsulfinylbenzylidene)-3-indenylacetic acid in an acetone solution.

Sources & evidence

ORD record
ord-f73a15126d6d4c4081f632c440550040
Source dataset
uspto-grants-1998_07
Patent number
US05776962

Reaction notes

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