HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Methoxy-1-Indanone → HCID 9862887, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Methoxy-1-Indanone | HCID 334036 | — |
| Reactant | 1-(Thien-2-ylcarbonyl)piperazine | HCID 797562 | — |
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Catalyst | Titanium isopropoxide | HCID 11026 | — |
| Product | HCID 9862887 | HCID 9862887 | — |
Reaction Steps
The title compound was prepared by the above procedure using 6-methoxy-1-indanone (2.6 g, 13.2 mmol), 1-(2-thienylcarbonyl)piperazine (2.1 g, 13.2 mol), titanium(IV) isopropoxide (5 mL, 15 mmol) and sodium borohydride (2.7 g, 67 mmol) to give 1.5 g of product as the fumarate salt.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05780470 |
| Source dataset | uspto-grants-1998_07 |
| ORD ID | ord-0233c621d70c4fd5af7f691f07d0ad2d |
| Source note | uspto-grants-1998_07 |