Thionyl Chloride → HCID 14985095, compound

HRID 1956331Notes

Reaction equation

HRID 1956331 reaction equation
[CH2:1]([C:4]1[CH:9]=[CH:8][C:7]([C:10]2[CH:18]=[CH:17][C:13]([C:14](O)=[O:15])=[CH:12][CH:11]=2)=[CH:6][CH:5]=1)[CH2:2][CH3:3].S(Cl)([Cl:21])=O>C(Cl)Cl>[CH2:1]([C:4]1[CH:9]=[CH:8][C:7]([C:10]2[CH:18]=[CH:17][C:13]([C:14]([Cl:21])=[O:15])=[CH:12][CH:11]=2)=[CH:6][CH:5]=1)[CH2:2][CH3:3]

Participants

4

Reactant 2

HCID 24386Thionyl ChlorideHCID 5228914-(4-Propylphenyl)benzoic Acid

Product 1

HCID 14985095HCID 14985095, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

A mixture of 2.0 g of 4-(4-propylphenyl]benzoic acid and 30 ml of thionyl chloride is stirred at reflux for 45 minutes. The reaction mixture is evaporated in vacuo to a residue which is evaporated from carbon tetrachloride (2×50 ml) to give a residue which is dissolved in methylene chloride.

Workup

  1. temperatureat reflux for 45 minutes
  2. customThe reaction mixture is evaporated in vacuo to a residue which
  3. customis evaporated from carbon tetrachloride (2×50 ml)
  4. customto give a residue which

Sources & evidence

ORD record
ord-52f7bcafe5734851bda203c84335a920
Source dataset
uspto-grants-1998_07
Patent number
US05780471

Reaction notes

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