HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 14985095, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 4-(4-Propylphenyl)benzoic Acid | HCID 522891 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 14985095 | HCID 14985095 | — |
Reaction Steps
A mixture of 2.0 g of 4-(4-propylphenyl]benzoic acid and 30 ml of thionyl chloride is stirred at reflux for 45 minutes. The reaction mixture is evaporated in vacuo to a residue which is evaporated from carbon tetrachloride (2×50 ml) to give a residue which is dissolved in methylene chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05780471 |
| Source dataset | uspto-grants-1998_07 |
| ORD ID | ord-52f7bcafe5734851bda203c84335a920 |
| Source note | uspto-grants-1998_07 |