HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chloro-3-ethoxy-2-methyl-1,8-naphthyridine → HCID 178465835, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chloro-3-ethoxy-2-methyl-1,8-naphthyridine | HCID 19374266 | — |
| Reactant | HCID 178507770 | HCID 178507770 | — |
| Product | HCID 178465835 | HCID 178465835 | — |
Reaction Steps
A mixture of 5-chloro-3-ethoxy-2-methyl-1,8-naphthyridine (2.0 g), 5-aminopyridin-2-ol (1.0 g) and IMS (20 ml) was boiled under reflux for 2 hours. The mixture was cooled and filtered to give 5-(3-ethoxy-2-methyl-1,8-naphthyridin-5-ylamino)pyridin-2-ol hydrochloride sesquihydrate, m.p. 295°-300° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05780482 |
| Source dataset | uspto-grants-1998_07 |
| ORD ID | ord-246f9b92ffbd487d855ea5f66ee7c6ec |
| Source note | uspto-grants-1998_07 |