HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenol → HCID 18663603, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | 2-Fluoro-4-(trifluoromethyl)benzaldehyde | HCID 522929 | — |
| Product | HCID 18663603 | HCID 18663603 | 78% |
Reaction Steps
Preparation analogous to Example 12 from 2-fluoro-4-trifluoromethyl-benzaldehyde and phenol. Yield: 78%, light-coloured crystals, crystallised from hexane; melting point: 57°-59° C.; TLC (silica gel; ethyl acetate/hexane=1:1; UV): Rf =0.71; 1H-NMR (CDCl3, 200 MHz): 7.08-7.50 (m, 7H): 8.05 (d, 1H) 10.60 (s, 1H). MS: 266/265 (M+), 217, 188.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05780500 |
| Source dataset | uspto-grants-1998_07 |
| ORD ID | ord-1b22085b821d409f9305f188870330ab |
| Source note | uspto-grants-1998_07 |