Pyrrolidine → HCID 18663595, compound

Participants

Reaction Steps

Preparation analogous to Example 2 from 10-bromomethyl-7-chloro-dibenz[b,f]oxepine and pyrrolidine. Yield: 5%, melting point:>225° C. decomposition. 1H-NMR (CD3OD, 200 MHz): 1.95-2.20 (m, 4H); 3.25 (m 2H); 3.55 (m, 2H), 4.52 (s, 2H), 7.20-7.45 (m, 7H); 7.60 (d, 1H). MS: 311 (M+, free base), 244, 242, 241, 215, 205, 178, 176, 163, 152.

Provenance & Evidence