HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorotrifluoroethylene → HCID 18663608, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorotrifluoroethylene | HCID 6594 | — |
| Reactant | HCID 18663609 | HCID 18663609 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 18663608 | HCID 18663608 | 99% |
Reaction Steps
Preparation analogous to Example 12 f) from 6-bromo-dibenz[b,f]oxepine-10-carboxylic acid. Yield: 99% crude, brown oil; TLC (silica gel; hexane/ethyl acetate=7.3; UV): Rf =0.07; 1H-NMR (CDCl3, 200 MHz): 3.54 (s, 2H), 6.70-7.49 (m, 8H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05780500 |
| Source dataset | uspto-grants-1998_07 |
| ORD ID | ord-235e06343eac43bf94d669ed55fd2930 |
| Source note | uspto-grants-1998_07 |