Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | Phenyl isocyanate | HCID 7672 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | Phenylurea | HCID 6145 | — |
Reaction Steps
To a solution of phenyl isocyanate (1.0 equiv.) in dimethyl formamide (1 mL) the corresponding aniline (1.0 equiv.) was added. The reaction mixture was stirred at about 80° C. until complete (24-48 hours), then the solvent was removed under vacuum. The purifications, yields and spectral characteristics for each individual compound are listed below.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05780483 |
|---|
| Source dataset | uspto-grants-1998_07 |
|---|
| ORD ID | ord-c960957765c64c04b47f8e5964ab3818 |
|---|
| Source note | uspto-grants-1998_07 |
|---|
