HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylbenzoyl Chloride → HCID 22951202, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylbenzoyl Chloride | HCID 13405 | — |
| Reactant | 6-Methoxy-2-(4-methoxyphenyl)benzo[b]thiophene | HCID 850941 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Product | HCID 22951202 | HCID 22951202 | 66.1% |
Reaction Steps
In a manner similar to that used in Preparation 3, 2.32 g (15 mmol) of 4-methylbenzoyl chloride, 2 g (7.4 mmol) of 2-(4-methoxyphenyl)-6-methoxybenzo[b]thiophene, and 5.3 g (40 mmol) of AlCl3 were converted to 1.9 g of the title compound, crystallized from Et2O and isolated as a light yellow powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05780648 |
| Source dataset | uspto-grants-1998_07 |
| ORD ID | ord-64847e78610948d5846852fef1372b26 |
| Source note | uspto-grants-1998_07 |