HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1956821Generated: October 29, 2026
Azobisisobutyronitrile → HCID 86752911, compound
https://huagongshe.com/reaction/1956821
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Azobisisobutyronitrile | HCID 6547 | — |
| Reactant | Thiophenol | HCID 7969 | — |
| Reactant | 1873-92-3 | HCID 74641 | — |
| Product | HCID 86752911 | HCID 86752911 | 88% |
Reaction Steps
26.8 g thiophenol, 18.8 g allyl (methyl) dichlorosilane and 0.60 mg azobisisobutylonitrile were put in a 100-mL three-neck flask that had been subjected to nitrogen substitution and the mixture was heated at 60° C. for 5 hours. After the reaction, the product was distilled under reduced pressure, obtaining 3-(thiophenyl) propyl (methyl) dichlorosilane with a 88% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05780661 |
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| Source dataset | uspto-grants-1998_07 |
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| ORD ID | ord-7b2980dbc6644da791257e99fba04db0 |
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| Source note | uspto-grants-1998_07 |
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