反应详情

To a solution of 4-(3-thienyl)toluene (3.56 g, 20.5 mmol) in carbon tetrachloride (100 ml) is added N-bromosuccinimide (3.64 g, 20.5 mol) and benzoyl peroxide (80 mg, 3.3 mmol). The reaction mixture is heated at reflux for 24 hrs. and concentrated in vacuo. The reaction mixture is recrystallized from ethanol to afford 4-(3-thienyl)benzyl bromide.

1. temperatureThe reaction mixture is heated
2. temperatureat reflux for 24 hrs
3. concentrationand concentrated in vacuo
4. customThe reaction mixture is recrystallized from ethanol