HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 19068972, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | HCID 14918455 | HCID 14918455 | — |
| Product | HCID 19068972 | HCID 19068972 | 78% |
Reaction Steps
Prepared from POCl3 (1.7 ml), DMF (1.6 ml), 1,5-dimethyl-1,3-dihydroindol-2-one (1.0 g) yielding (46) 1.0 g (78%). M.p. 120°-121° C. as crude product sufficiently pure for the next synthesis.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05783575 |
| Source dataset | uspto-grants-1998_07 |
| ORD ID | ord-f28cd284fe8542e1b7843fb7468a8b54 |
| Source note | uspto-grants-1998_07 |