HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54347391, compound → HCID 19069372, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54347391 | HCID 54347391 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 19069372 | HCID 19069372 | — |
Reaction Steps
Using the alcohol prepared above and the procedures described in Example 84E, except chromatography using 4:1 hexane-EtOAc was used for purification, provided 4-(thiazol-2-yloxy)benzaldehyde. 1H NMR (CDCl3) δ10.00 (s, 1H), 7.95 (m, 2H), 7.46 (m, 2H), 7.30 (d, 1H), 6.95 (d, 1H). MS (DCl/NH3) (M+H)+ 206 and (M+H+NH3)+ 223.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05783593 |
| Source dataset | uspto-grants-1998_07 |
| ORD ID | ord-008a5b366ced45e5b5e15f0af330ec28 |
| Source note | uspto-grants-1998_07 |