Aluminium lithium hydride → HCID 57075766, compound

Participants

Reaction Conditions

Reaction Steps

The butylamine prepared above (57 mg, 0.21 mmol) in THF (1 mL) at room temperature was treated with 1M LAH in THF (0.42 mL). The solution was warmed to reflux for 4 hours, cooled to 0° C. and quenched with sodium sulfate decahydrate. The slurry was filtered through celite and concentrated to provide 53 mg (99%) of the title compound as a colorless oil.

Provenance & Evidence