HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Pyridinecarboxaldehyde → HCID 54560653, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Pyridinecarboxaldehyde | HCID 10371 | — |
| Reactant | 4-amino-4,5-dihydro-1H-1,2,4-triazol-5-one | HCID 567624 | — |
| Catalyst | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 54560653 | HCID 54560653 | — |
Reaction Steps
A mixture of 4 g of 4-amino-1,2,4-triazol-3-one and 100 ml of alcohol is heated to the reflux temperature and 4.3 g of pyridine-3-carbaldehyde and 2 drops of 6N hydrochloric acid are added thereto. After 30 minutes under reflux the reaction mixture is cooled to 20°. The product that has precipitated is then filtered off with suction and dried under a high vacuum. 4.6 g of the title compound having a melting point of 264°-265° are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05783704 |
| Source dataset | uspto-grants-1998_07 |
| ORD ID | ord-dc30621c02424c168035bbb5f4125e6f |
| Source note | uspto-grants-1998_07 |