Thionyl Chloride → HCID 19068257, compound

HRID 1957700Notes

Reaction equation

HRID 1957700 reaction equation
[C:1]12([C:11]3[CH:12]=[C:13]([CH:17]=[CH:18][C:19]=3[O:20][CH2:21][C:22]([O:24][CH3:25])=[O:23])[C:14](O)=[O:15])[CH2:10][CH:5]3[CH2:6][CH:7]([CH2:9][CH:3]([CH2:4]3)[CH2:2]1)[CH2:8]2.S(Cl)([Cl:28])=O>>[C:1]12([C:11]3[CH:12]=[C:13]([CH:17]=[CH:18][C:19]=3[O:20][CH2:21][C:22]([O:24][CH3:25])=[O:23])[C:14]([Cl:28])=[O:15])[CH2:10][CH:5]3[CH2:6][CH:7]([CH2:9][CH:3]([CH2:4]3)[CH2:2]1)[CH2:8]2

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 19068275HCID 19068275, compound

Product 1

HCID 19068257HCID 19068257, compound

Procedure

1.78 g (5 mmol) of 3-(1-adamantyl)-4-methoxycarbonylmethyloxybenzoic acid and 15 ml of thionyl chloride were introduced into a round-bottomed flask and the mixture was heated at reflux for one hour. It was evaporated to dryness and the crude acid chloride, which was used without further purification in the remainder of the synthesis, was recovered.

Workup

  1. temperaturethe mixture was heated
  2. temperatureat reflux for one hour
  3. customIt was evaporated to dryness
  4. customthe crude acid chloride, which was used without further purification in the remainder of the synthesis
  5. customwas recovered

Sources & evidence

ORD record
ord-e9dc5cf1ad6946c182f2aee6b3dfe0dc
Source dataset
uspto-grants-1998_07
Patent number
US05786379

Reaction notes

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